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1.
China Journal of Chinese Materia Medica ; (24): 1108-1113, 2015.
Article in Chinese | WPRIM | ID: wpr-246142

ABSTRACT

An investigation on the chemical constituents of the 90% EtOH extract of Perovskia atriplicifolia led to the isolation of fifteen compounds from the EtOAc fraction. Based on the detailed spectral analysis (MS, 1D and 2D NMR), as well as comparison with the literatures, the structures of compounds 1-15 were determined as cirsimaritin (1), salvigenin (2), syringaldehyde (3), vinyl caffeate (4), 2α, 3α-dihydroxyolean-12-en-28-oicacid (5), 2α, 3α-dihydroxyurs-12-en-28-oicacid (6), niga-ichigoside F1 (2α, 3β, 19α, 23- tetrahydroxyurs - 12-en-28-oicacid- O-β-D- glucopyranoside, 7), sericoside (8), 4-epi-niga-ichigoside F1 (2α, 3β, 19α, 24-tetrahydroxyurs-12-en-28-oicacid O-β-D-glucopyranoside, 9), 2α, 3β, 24-trihydroxyolean-12-en-28-oicacid O-β-D-glucopyranosyl-(1 --> 2) - β-D-glucopyranoside (10), pruvuloside A (11), asteryunnanoside A [2α, 3β, 23-trihydroxyolean-12-en-28-oicacid O-β-D-glucopyranosyl-(1 --> 2)-β- D- glucopyranoside,12], rosmarinic acid methyl ester (13), β-sitosterol (14), and daucosterol (15), respectively. Compounds 1-13 were isolated from the Perovskia genus for the first time. All the compounds were obtained from P. atriplicifolia for the first time.


Subject(s)
Drugs, Chinese Herbal , Chemistry , Lamiaceae , Chemistry , Magnetic Resonance Spectroscopy , Molecular Structure , Spectrometry, Mass, Electrospray Ionization
2.
China Journal of Chinese Materia Medica ; (24): 500-503, 2007.
Article in Chinese | WPRIM | ID: wpr-283447

ABSTRACT

<p><b>OBJECTIVE</b>To study the chemical constituents of Cynanchum forrestii.</p><p><b>METHOD</b>Chromatographic techniques were applied to isolated chemical constituents. The structures were identified on the basis of physico-chemical constants and spectroscopic data.</p><p><b>RESULT</b>Eight compounds were isolated from the 95% ethanol extract of the roots of C. forrestii and elucidated as ( + ) -5'-methoxyisolariciresinol 3a-O-beta-D-glucopyranoside (1), hexahydroxycholest-7-en-6-one (2), tylophorinidine (3), sucrose (4), palmitic acid (5), beta-sitosterol (6), daucosterol (7), nonanedioic acid (8).</p><p><b>CONCLUSION</b>Compounds 1-3 from this genus, and compounds 4-8 from the plant were obtained for the first time.</p>


Subject(s)
Alkaloids , Chemistry , Cholestenones , Chemistry , Cynanchum , Chemistry , Glucosides , Chemistry , Isoquinolines , Chemistry , Palmitic Acid , Chemistry , Plant Roots , Chemistry , Plants, Medicinal , Chemistry
3.
China Journal of Chinese Materia Medica ; (24): 599-603, 2007.
Article in Chinese | WPRIM | ID: wpr-283425

ABSTRACT

<p><b>OBJECTIVE</b>To study the chemical constituents from the roots of Craibiodendron henryi.</p><p><b>METHOD</b>Various chromatographic techniques were used to isolate and purify the constituents. The structures were elucidated by chemical evidence and spectral methods.</p><p><b>RESULT</b>Twelve compounds were isolated from the ethyl acetate soluble fraction of the 95% ethanolic extract and their struc- tures were elucidated as quercetin (1), quercetin-3-O-rhamnicoside (2), quercetin-3-O-arabinofuranoside (3), (-)-epicatechin (4), proanthocyanidin A-2 (5), procyanidin B-2 (6), (-)-isolariciresinol-2a-O-beta-D-xylopyranoside (7), lyoniside (8), sitoster-yl-3beta-glucoside-6'-O-palmitate (9), beta-sitosterol (10), daucosterol (11) and octacosanoic acid (12).</p><p><b>CONCLUSION</b>Compounds 1-12 were isolated from this plant for the first time.</p>


Subject(s)
Biflavonoids , Chemistry , Catechin , Chemistry , Ericaceae , Chemistry , Molecular Structure , Plant Roots , Chemistry , Plants, Medicinal , Chemistry , Proanthocyanidins , Chemistry , Quercetin , Chemistry , Sitosterols , Chemistry
4.
China Journal of Chinese Materia Medica ; (24): 1544-1604, 2007.
Article in Chinese | WPRIM | ID: wpr-287918

ABSTRACT

<p><b>OBJECTIVE</b>To study the chemical constituents from the leaves of Acer truncatum.</p><p><b>METHOD</b>Various chromatographic techniques were used to isolate and purify the constituents. The structures of these compounds were elucidated on the basis of spectral analysis.</p><p><b>RESULT</b>Seven compounds were isolated and identified as p-sitosterol (1), beta-amyrin (2), beta-amyrin acetate (3), 3, 5-dihydroxy-4-methoxybenzoic acid (4), astragalin (5), quercetin-3-O-beta-D-galactoside (6), and quercetin-3-O-alpha-L-rhamnoside (7).</p><p><b>CONCLUSION</b>All of compounds were isolated from this plant for the first time.</p>


Subject(s)
Acer , Chemistry , Gallic Acid , Chemistry , Kaempferols , Chemistry , Oleanolic Acid , Chemistry , Plant Leaves , Chemistry , Plants, Medicinal , Chemistry
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